Sample: ZX30_5pct_TD200_AS-DEF

Ungroup Processes

Last Updated: 2 weeks ago Owner: Tracy Berman ID: 78869
EBSD (7)
Settings
Scan date:
2/14/24
Scan date:
2/15/24
Scan date:
5/16/24
SEM view field width:
550 µm
SEM view field width:
2200 µm
Scan Width:
400 µm
Scan Width:
300 µm
Scan Width:
200 µm
Scan Width:
2000 µm
Scan Height:
250 µm
Scan Height:
400 µm
Scan Height:
200 µm
Scan Height:
1000 µm
Step size:
5 µm
Step size:
0.15 µm
Step size:
0.5 µm
Step size:
1 µm
frames per second:
70 fps
frames per second:
66 fps
EBSD Camera Binning:
1 x 1
Background setting:
standard
Background setting:
enhanced
Grid type:
hexagonal
Grid type:
square
Final Polishing Step:
fumed Si
Final Polishing Step:
1 µm diamond paste
CI>0.1 after rescan:
0.911
CI>0.1 after rescan:
0.891
Voltage:
30 kV
Voltage:
30 kV
Beam Intensity or current:
20
Beam Intensity or current:
20
Measurements
% points with CI>0.1:
0.743
% points with CI>0.1:
0.781
% points with CI>0.1:
0.83
Alloy:
ZX30
Average dislocation density:
9.3*10^13
Average dislocation density:
1.1*10^14
Average dislocation density:
9.7*10^13
Unloaded strain:
4%
Composition Zn content:
3.03 wt%
Total Fraction Less than 1º:
1.2 %
Total Fraction Less than 1º:
3.4 %
Total Fraction Less than 1º:
1.4 %
Composition Ca content:
0.096 wt%
Number of grains:
228
Number of grains:
462
Number of grains:
208
Average Diameter:
18 µm
Average Diameter:
17.2 µm
Average Diameter:
18.5 µm
Twin fraction:
19.7
Twin fraction:
0.132
Files
Gleeble (1)
Settings
Test Date:
2/6/24
Testing Mode:
PSC
Initial height or thickness:
10 mm
Initial width:
15.08 mm
Initial length:
19.97 mm
Final height or thickness:
9.57 mm
Final length:
20.17 mm
Pre-deformation soak Temp:
200 ºC
Deformations:
1
Initial Strain Rate:
0.5 /s
Strain Per pass:
0.05
Stage One - Temp during Deformations:
200 ºC
Quench Duration:
45 s
:
heating fluctuated alot (190 to 210), but SS curve looks consistent
Rate to Temp:
5 ºC/s
Program Strain Type:
TRUE
Pre-deformation Soak Time:
600 s
Specimen orientation:
CD || ED
Measurements
% points with CI>0.1:
0.743
% points with CI>0.1:
0.781
% points with CI>0.1:
0.83
Alloy:
ZX30
Average dislocation density:
9.7*10^13
Average dislocation density:
1.1*10^14
Average dislocation density:
9.3*10^13
Unloaded strain:
4%
Composition Zn content:
3.03 wt%
Total Fraction Less than 1º:
1.4 %
Total Fraction Less than 1º:
3.4 %
Total Fraction Less than 1º:
1.2 %
Composition Ca content:
0.096 wt%
Number of grains:
462
Number of grains:
228
Number of grains:
208
Average Diameter:
17.2 µm
Average Diameter:
18.5 µm
Average Diameter:
18 µm
Twin fraction:
19.7
Twin fraction:
0.132
Files
GND Calculation (3)
Measurements
% points with CI>0.1:
0.83
% points with CI>0.1:
0.781
% points with CI>0.1:
0.743
Alloy:
ZX30
Average dislocation density:
9.3*10^13
Average dislocation density:
1.1*10^14
Average dislocation density:
9.7*10^13
Unloaded strain:
4%
Composition Zn content:
3.03 wt%
Total Fraction Less than 1º:
1.4 %
Total Fraction Less than 1º:
3.4 %
Total Fraction Less than 1º:
1.2 %
Composition Ca content:
0.096 wt%
Number of grains:
208
Number of grains:
462
Number of grains:
228
Average Diameter:
18.5 µm
Average Diameter:
18 µm
Average Diameter:
17.2 µm
Twin fraction:
19.7
Twin fraction:
0.132
Files
Receive Samples (1)
Settings
Receipt Date:
4/28/22
Source:
CanMET
Solution treatment time:
1 hr
Solution treatment Temp:
325 ºC
Measurements
% points with CI>0.1:
0.743
% points with CI>0.1:
0.781
% points with CI>0.1:
0.83
Alloy:
ZX30
Average dislocation density:
9.3*10^13
Average dislocation density:
1.1*10^14
Average dislocation density:
9.7*10^13
Unloaded strain:
4%
Composition Zn content:
3.03 wt%
Total Fraction Less than 1º:
1.4 %
Total Fraction Less than 1º:
3.4 %
Total Fraction Less than 1º:
1.2 %
Composition Ca content:
0.096 wt%
Number of grains:
228
Number of grains:
208
Number of grains:
462
Average Diameter:
18 µm
Average Diameter:
18.5 µm
Average Diameter:
17.2 µm
Twin fraction:
0.132
Twin fraction:
19.7
Files