Dataset: The dynamics of recrystallized grains during static recrystallization in a hot-compressed Mg-3.2Zn-0.1Ca wt.% alloy using in-situ far field high-energy diffraction microscopy

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Published: 3 years ago Views: 522 Downloads: 148 DOI: 10.13011/m3-my0r-vg37 License: Attribution License (ODC-By) Size: 523.75 MB
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The dynamics of recrystallized grains during static recrystallization in a hot-compressed Mg-3.2Zn-0.1Ca wt.% alloy using in-situ far field high-energy diffraction microscopy 17
  • Reza Roumina
  • Sangwon Lee
  • Tracy Berman
  • John Allison
  • Ashley Bucsek

The poor formability of rolled magnesium (Mg) alloy sheet remains a barrier to its widespread commercial use and is attributed to the strong basal texture that occurs in most mechanically processed Mg alloys. Recent attempts to successfully weaken the texture have been made using Mg-Zn-Ca alloys in combination with post-deformation annealing. The motivation for this work is to understand the evolution of the mesoscale processes that occur during annealing (specifically, static recrystallization) and lead to this texture weakening. Toward this goal, more than 1,200 recrystallized grains were studied during in-situ annealing in an 80% hot-compressed Mg-3.2Zn-0.1Ca wt.% (ZX30) alloy using far-field high-energy diffraction (ff-HEDM). The relative volume, crystallographic orientation, and position of each recrystallized grain emerging within a 1×1×0.1 mm3 volume were tracked throughout static recrystallization. These measurements were used to quantitatively measure the nucleation and growth statistics associated with recrystallized grains as a function of annealing time. The measurements reflected a highly heterogeneous process with individual grain dynamics varying wildly from the average, and they also point to relations between relative grain volume and growth rate (or more accurately, the rate of change of relative grain volume) with a peak average rate occurring early in recrystallization (at 22% recrystallized). We also explore whether a recrystallized grain's current state can be used to predict its future growth behaviors with implications for Monte Carlo simulations. Finally, we investigate whether recrystallized grains with specific orientations have preferential nucleation and/or growth, and we find that grains with a weak basal texture have a pronounced nucleation advantage that increases with annealing time, while other grain orientations have a slight growth advantage that diminishes with annealing time.

This work was supported by the U.S. Department of Energy Office of Basic Energy Sciences Division of Materials Science and Engineering under Award #DE-SC0008637 as part of the Center for PRedictive Integrated Structural Materials Science (PRISMS). This work is based upon research conducted at the Cornell High Energy Synchrotron Source (CHESS) which is supported by the National Science Foundation under award DMR-1829070.

  • The dynamics of recrystallized grains during static recrystallization in a hot-compressed Mg-3.2Zn-0.1Ca wt.% alloy using in-situ far field high-energy diffraction microscopy
    Roumina, R., Lee, S., Berman, T. D., Shanks, K. S., Allison, J. E., & Bucsek, A. (2022). The dynamics of recrystallized grains during static recrystallization in a hot-compressed Mg-3.2Zn-0.1Ca wt.% alloy using in-situ far field high-energy diffraction microscopy. Acta Materialia, 234, 118039. https://doi.org/10.1016/j.actamat.2022.118039
    https://doi.org/10.1016/j.actamat.2022.118039
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