Oxidation Isothermal Exposure - 0.5h (1)

Cooling Rate:

No value

Time:

0.5 h

Cooling Type:

{ "name": "Gas Cooled", "value": "gas_cooled" }

Temperature:

800 C

Sectioning (1)

Notes:

Sectioned output samples using slow speed diamond saw

SEM (1)

Voltage:

5 kV

Stage:

{ "name": "Standard", "value": "standard" }

Specimen/Stage Bias:

No value V

Current:

0.4 nA

Working Distance:

4 mm

Detector:

{ "name": "Secondary", "value": "secondary" }

Stage Tilt:

No value degrees

Magnification:

15000

Files

• SEM - Surface Oxide - Pure Ti, 0.5 hour oxidation, 800C, 20% O2 - 15 kx - 9-15-2016.tif
  

STEM EDS (1)

Camera Length:

No value

Voltage:

200 kV

Scanning:

No value

Conventional Scanning:

{ "name": "Yes", "value": "yes" }

Apparatus:

Hitachi HD-2300 Scanning Transmission Electron Microscope

Stage:

{ "name": "Standard", "value": "standard" }

Spot Size:

No value

Mode:

{ "name": "Scanning z-contrast", "value": "scanning_z_contrast" }

Files

• STEM EDS - Pure Ti, 0.5 hour oxidation, 800C, 20% O2 - O EDS Map.tif
  
• STEM EDS - Pure Ti, 0.5 hour oxidation, 800C, 20% O2 - Pt EDS Map.tif
  
• STEM EDS - Pure Ti, 0.5 hour oxidation, 800C, 20% O2 - Ti EDS Map.tif
  
• STEM Z Contrast - Pure Ti, 0.5 hour oxidation, 800C, 20% O2.TIF
  

TEM (1)

Camera Length:

No value

Apparatus:

JEOL 2010F AEM

Conventional Scanning:

{ "name": "Yes", "value": "yes" }

Mode:

{ "name": "Diffraction Imaging", "value": "diffraction_imaging" }

Scanning:

{ "name": "Bright Field", "value": "bright_field" }

Voltage:

200 kV

Stage:

{ "name": "Standard", "value": "standard" }

Spot Size:

No value

Files

• Bright Field TEM - Pure Ti, 0.5 hour oxidation, 800C, 20% O2 - 10-13-2016.tif