Hardness Profiles (1)

Type:

No value

Load:

0.001 N

Dwell Time:

2 s

Files

• Nanoindentation Hardness Profiles - Pure Ti and Oxidized Ti Samples with and without Si coating.tif
  

Oxidation Isothermal Exposure - 2h (1)

Cooling Type:

{ "name": "Gas Cooled", "value": "gas_cooled" }

Temperature:

800 C

Cooling Rate:

No value

Time:

2 h

Sectioning (1)

Notes:

Sectioned output samples using slow speed diamond saw

SEM (1)

Current:

0.4 nA

Detector:

{ "name": "Secondary", "value": "secondary" }

Working Distance:

4 mm

Stage:

{ "name": "Standard", "value": "standard" }

Stage Tilt:

No value degrees

Voltage:

5 kV

Magnification:

15000

Specimen/Stage Bias:

No value V

Files

• SEM - Surface Oxide - Pure Ti, 2 hr oxidation, 800C, 20% - 15kx - 8-2-2016.tif
  

TEM (1)

Conventional Scanning:

{ "name": "Yes", "value": "yes" }

Mode:

{ "name": "Diffraction Imaging", "value": "diffraction_imaging" }

Spot Size:

No value

Voltage:

200 kV

Camera Length:

No value

Scanning:

{ "name": "Bright Field", "value": "bright_field" }

Apparatus:

JEOL 2010F

Stage:

{ "name": "Standard", "value": "standard" }

Files

• Bright Field TEM - Pure Ti, 2 hour oxidation, 800C, 20% O2 - 8-22-2016.tif